Golterman,H.L.(1996): Fractionation of sediment phosphate with chelating compounds: a simplification, and comparison with other methods. Hydrobiologia, 335, 87-95.

『キレート剤を用いた堆積物リン酸塩の分別:単一化および他の方法との比較』


Abstract
 The NTA/EDTA fractionation of sediment-bound, inorganic phosphate was improved and made more effective. The iron-bound phosphate is now extracted with Ca-EDTA plus dithionite and followed by an extraction of calcium-bound phosphate by Na2-EDTA at pH = 4.5. A comparison is made with two other sequential extraction procedures: the SEDEX and the Hieltjes & Lijklema extractions. The EDTA extractions have an advantage over the other two methods.』

Abbreviations

 ASOP = Acid Soluble Organic Phosphate
 CaCO3−P = calcium-bound phosphate
 EDTA = Ethylene dinitrilo tetraacetic acid (or its salts)
 Fe(OOH)−P = iron-bound phosphate
 M = mol dm-3
 NaOH-Pextr = phosphate extracted with NaOH (etc.)
 NTA = Nitrilo triacetic acid (or its salts)
 o-P = ortho phosphate
 TRIS-buffer = tris (hydroximethyl)-amino methane

Introduction
Methods
Results
Discussion
Comparison between old and new NTA/EDTA methods
Comparison of different methods
Acknowledgments
References
Annex 1
Protocol
Annex 2


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